Monday, February 13, 2023

Rotoforge 2/13/2023

Today we solved two major problems at once... 

1.) We finally managed to find a liner material that survives during extrusion and is extremely effective at preventing welding between the wire feed stock and the motor shaft walls. This welding was previously responsible for nonrecoverable jamming and welding of multiple motors...

 2.) We finally managed to eliminate "candy caning" as seen in the figure below, completely. That is the shear coupling between the wire feed stock and the rotating die has been eliminated without eliminating the energy transfer between the tip of the wire and the inside surface of the die that facilitates frictional heating and extrusion of the wire onto the build plate. this was previously responsible for breaking the feedstock off inside the shaft and causing jams... In short, lubrication and higher RPM helped with this point.

Figure 1.) showing the candy caning of previous iterations of rotoforge wire feed stock... the twisting force imparted due to the force of friction at lower RPM and higher feedstock pressure causes greater shear coupling between the fluidized metal in the die and the rest of the feedstock, this causes twisting and often breakage which results in a jam.

As it turns out conventional motor oil, particularly heavier grades such as 10W-40 and 15W-40 full synthetic contain pressure and shear sensitive additives for reducing wear and oil film disruption such as ZDDP. These additives in tandem with a robust, heat and abrasion resistant mechanical barrier, such as E-glass fiber, provides for an excellent high speed, high temperature tolerant bearing between the metal wire feedstock and the walls of the rotating shaft. This next section includes some points of theory, and may be a little techy so I will try to provide some explanatory graphics and easily referenceable sources for guidance.

 1.) this paper, and a few others provide information on the requirements to print aluminum in the solid state. Their stated operating parameters were:

  • 1000 RPM
  • Ram force (extruder pressure) = 10 -21 MPa
  • layer thickness of 1 millimeter
  • track width of 20 millimeters
  • D_f = Feed rod diameter of 15.9 millimeters, A_f, cross sectional area of  198.56 square millimeters
  • A_n =Die orifice (nozzle exit area) 70 square millimeters
  • Die orifice length of ~10 mm
  • the extrusion ratio, or the ratio of nozzle exit area to feed rod cross sectional area is ~2.84
  • This indicates a nozzle exit diameters of ~9.4 millimeters
  • A surface area to volume ratio at their die orifice of ~2.42
  • A characteristic working volume of  >= 582.56 cubic millimeters

    In our present iteration of Rotoforge, our accessible printing parameters are thus
  •  29,000 RPM
  • Ram force (extruder pressure) = 7-15 MPa
  • layer thickness of ~0.1 millimeters
  • track width of ~ 2 millimeters
  • D_f = feed rod diameter of ~1.6 millimeters, A_f, cross sectional area of 2.01 square millimeters
  • A_n = Die orifice(nozzle exit area) of 0.717 square millimeters
  • Die orifice length of ~1 mm
  • for the same extrusion ratio as above, this corresponds to a nozzle exit diameter of 0.95 millimeters
  • Our resulting surface area to volume ratio would be ~6.17
  • a characteristic working volume 5.727 cubic millimeters

Before we consider anything more complicated, such as the specific behavior of dry or lubricated metal on metal friction at low sliding speeds (1-20 m/s), a few important features stand out from comparison of their parameters to ours. 

  • 6.17 : 2.42 ratio of surface area to volume ratio implies a ~ 2.5 X larger loss path for heat conduction away from the volume of worked material in the die orifice, on the build plate and inside the feed stock above the die for Rotoforge... this is a point against us in terms of ease of flowing material due to the greater loss of heat generated by friction between the feedstock and the rotating die, but a point for us in terms of die longevity and system thermal control. this also implies that our system could sustain higher proportional mass flow rates while staying in the thermal envelope of the materials used in the die, and other components.

  • 582.56 : 5.727 cubic millimeters volume ratio implies ~100X smaller heat generation due to volume plastic deformation in Rotoforge versus large scale commercial systems.  This again is a point against us in terms of material being flowable, since the total heat evolved is smaller, the feedstock material will generally remain at a lower temperature for a given amount of input energy from friction between the feedstock and the rotating die. this is largely negated by the fact that the total volume, and thus mass of feedstock to heat is also smaller by the same 100X factor.   This bodes well for thermal management as it reduces the total waste heat that must be dissipated from the system to maintain the same proportional mass flow rate of feedstock through the die.

  • With nothing but a guess at the length of the die orifice in the paper above, I cannot say for sure what our proportionate die orifice length should be, but I can guess that shorter is better to within the limits of the hot strength of the die materials as it reduces friction between die walls and extrudate and reduces total extruder pressure required to obtain a given mass flow rate.

  •  Ram force is in the same ball park... Rotoforge could probably do with a better extruder that is less prone to slippage and provides at least 25 MPa of pressure, or about 25 newtons / square millimeter... or for a 1.6mm diameter feed stock, an extruder capable of ~50-100 netwtons total force on the feedstock metal wire.
     
  • Without reference to non-extant exact theory, but with some papers for your perusal if you care for more details..  in general, the force of friction decreases with speed in soft metal - hard metal contacts. In effect, high shear rates and elevated temperatures due to friction, in the absence of welding, produce a situation like a metallic fluid bearing. This very imprecisely means that for our system specifically, between aluminum and stainless steel, the force of friction should decrease linearly with RPM, thus reducing the net shear strain on the wire feed stock away from the die-feed stock interface.
  •  Simultaneously, the energy released due to this sliding fluidized metal friction between metallic surfaces, scales as the surface velocity squared. given that our die orifice is ~2.7 mm in circumference, and is rotating at ~29,000 RPM, our effective surface speed at the orifice edge is 78,300 millimeters / minute, or approximately ~1.305 meters/second. The surface speed of the large commercial system at the die orifice is ~28,200 millimeters/minute, or approximately, ~0.433 meters/second. this means, comparatively, that our "frictional energy" is about 9X larger, per unit feed stock surface area,(due to 3X the surface velocity and the velocity square in the energy term) at the interface between our wire and die, than their rod and die assuming the same applied extruder pressure and assuming the same coefficient of friction (this is almost certainly false, but within an order of magnitude).   This means we should be in the ball park, in spite of the larger thermal loss paths and smaller volume, all other things equal, to print aluminum 6061-T6 with our current Rotoforge setup.
  • If we move to a more powerful and faster spinning off the shelf motor or belted offset spindle drive, at 60,000 RPM, we could obtain surface speeds at the orifice of ~2.8 meters / second, or about ~36X the surface friction energy of the large commercial system.  TLDR; more speed is better when it does not adversely effect longevity. cost or safety.  More input energy at the feed stock - die interface results in a lower feedstock viscosity, and a larger mass flow rate through the orifice for a constant extruder pressure.  

    So you might be wondering as I have, what is the holdup!?
    The answer seems relatively simple : Material confinement! 
In short, because the end of the wire is under pressure, at elevated temperature and shear rates, and is thus behaving as a fluid, it flows to fill the space available to it! 
Figure 2). You can see the expansion of the 1.6 mm diameter Al6061 feedstock to 2.2mm diameter foot, where it contacts the interior of the rotating die. 2.2mm is the internal diameter of the hollow motor shaft to which the die is tightly attached. The feed stock has expanded to fill the diameter of the hollow shaft, because it is unconstrained radially and so, once fluidized under pressure, flows through the path of least resistance(outward toward the walls with the centripetal force) until it fills its container.

This expansion of the end of the wire results in an increase in diameter to ~2.2-2.4 millimeters. This results in an increase of surface area to nearly ~4 square millimeters, thus cutting the pressure applied by our extruder at least in half.  Hence why the material can begin to flow, and then stop flowing once the pressure is reduced due to the larger area of contact.

Figure 3.) Initially the feedstock is a simple cylinder with a diameter of 1.6 mm and a surface area at the tip of ~2.01 mm squared. There are two flow paths available given the finite extruder pressure... once the feedstock is heated by friction and begins to flow, the extruder pressure and centripetal force cause it to flow into the open flow paths.

Given our limited pushing power, 14-30 netwons at most, dividing that force over twice the area easily brings us from ~7-15 megapascals of pressure to ~2-7 megapascals. Which is below the threshold flow stress for Aluminum 6061 at it's solidus of 595 celcius, and below the extrusion pressure used in the above paper, by a factor of at worst, 10X, and at best 1.5X ... we may have 9X the input energy per surface area of feed stock, but if that energy is spread over 2X as much area, and we lose 2.5 X as much energy to thermal dissipation, we would already be behind in terms of the viscosity of our feedstock(in response to the decreased energy density) at the die opening, despite this increased surface friction energy working for us.


Figure 4.) Once the feedstock has begun to flow into the die orifice and has filled the initially open flow paths, the extruder pressure decreases, as the force the extruder can apply is constant, but the bearing area of the end o the wire has increased in proportion to the square of its change in radius. now 2.2 mm in diameter, its effective surface area is ~4 square mm. This cuts the extruder pressure at least by half. Additionally, contact with the walls further increases this bearing area over which the extruder force is spread, thus further decreasing the pressure. To make this worse, the extrudate has its own bearing area to contribute, and a relatively large surface area on which friction in the die orifice can act. This increases the reaction forces substantially. Thus extrusion stops.

 Our next order of business will be producing a new die shape, that constrains the feed stock and prevents this expansion at the interface as much as possible, in order to force extrusion through the die opening preferentially without substantially increasing the area of contact. Additionally, an extruder upgrade is certainly in the cards.  A new offset spindle design capable of at least a sustained ~60,000 RPM  is probably a near term improvement as well. 

 

Figure 5.) The new Rotoforge tool design which will hopefully confine the fluidized metal to the interior of the die, and maintain a constant bearing area, so that the extrusion pressure can remain constant at constant extruder force, and the feedstock material can be continuously extruded.  Ideally the tip catch will hold a tight fit to the end of the wire, without introducing too much additional fricton, and when the wire expands and fluidizes at the tip, it will be captured in the catch and the material will have nowhere to go but through the orifice.

 Thanks for taking the time to read this far if you have! Looking forward to posting some real results in the next month!

Back to the lab!



Wednesday, February 1, 2023

Rotoforge 2/1/2023

Much has happened since my last post. I have provided all the neccessary CAD and CAM files, and complete bill of materials for Rotoforge on the github... and have provided a preliminary visual assembly guide on youtube. So far Rotoforge is not "working", but it is "kinda working" in that metal can be extruded for some length of time stabily and long enough that it can be deposited. I intend to compile and upload a few videos of the tests and experiments I have been running with various alloys and pure metals with tools that are generally made of a simple stainless steel acorn nut, with a hole drilled in their center. Like so
This is essentially the same operation as in the early days of the rep-rap project. Thus, Making nozzles from acorn nuts has been a long tradition. In our case however, their behavior is slightly different... and given the internal geometry of the acorn nuts compared to current conical nozzles on standard FDM printers, the acorn nuts, posessing a flat landing inside their apex are preferable for extrusion of metals and other high viscosity elements by shear and friction assistance.

Something I have found in my experiments, is that a concical converging nozzle section as in most FDM nozzles, presents a large change in surface area during the initial contact between a metal wire and the interior of the rotating nozzle. This results in a conical cross section of metal that must be plastically deformed before it exits at the final diameter of the nozzle orifice. A cone has much larger surface area (even more so at small diameters) than a flat disk. This effect can be seen in these experimental images of metal wires pressed in flat acorn nut interiors and into conical FDM nozzle interiors...

The approximate surface area of the conical converging FDM nozzle section is ~6 square millimeters while that of the flat acorn nut interior is ~2.4square millimeters. The represents almost a 3X reduction in surface area! and thus at least a 3X increase in effective pressure applied by our extruder!. Moreover, the reduction in surface area reduces the frictional force by a comparable factor. Though in classical approximations the frictional force does not depend on surface area, in more advanced physics of tribology we understand that the friction between two bodies depends on the real area of contact between them.

We can roughly approximate the area of contact in a worst case complete contact scenario, but knowing the real area of contact in practice for any set of materials with any set of surface conditions is impractical at this time. This is important for rotoforge, because the area of contact determines how much area, energy is transfered through from the rotation of the BLDC to the feed stock material. If the area is larger, the energy will be dissipated by a larger volume of material to work, and we will require more power to plasticize the material and make it flowable given the limit of force the extruder can exert. This means that a flat disk shaped interior is preferable because it reduces the required motor power and extruder force to provide a given mass flow of material through an orifice of known size. This has made a huge difference in ou ability to extrude metals through smaller orifices and thus in the resolution we can obtain with rotoforge as of late!

Additionally, the choice of feed stock alloy is incredibly important! Dead soft 1100 aluminum has very differnet properties from 6061 - T6 aluminum, and al aluminums are very different from copper and brass. In the case of rotoforge we have recently discovered that materials of greater alloy content, that is, they have more components in their overall mixture, are easier to work with generally and extrude more readily, particularly when their solidus is at a lower temperature, and when their temperature dependent flow stress and youngs modulus at any given temperature are lower. Additionally, lower melting point helps, but is not alway the only factor at play. In general, if a material is more "machineable" it will perform better in rotoforge. Extrudability of the alloy in conventional processes seems to have little bearing on how well it works for us at our scale. Of particular interest, is the difference in 1100, and 6061 aluminum... Recently we discovered that 6061 aluminum will happily extrude for many minutes at feed rates of up to 12 mm/ minute throgh our rotoforge tool. While 1100 will barely make it 1 minute before jamming and breaking at that feed rate. Both wires having a diameter of 1.65 mm OD on average. we have not yet honed in on exactly why this is, but we have some conjectures... In particular, that the lower thermal conductivity, lower solidus temperature, and larger overall strain to break and specific resilience of 6061 due to its larger number of alloying components lends it more desirable properties for printing, in addition to making it a stronger alloy overall.

Essentially, the combination of physical properties of 6061, including its ability to absorb more energy per unit volume without rupture, allows it to both more readily extrude through the orifice of our rotoforge "tool" (M5 Stainless steel acorn nut, and maintain the integrity of the feedstock material without breaking or twisting off inside the rotating motor shaft due to excessive shear strain buildup... this means that it can be fed at a continuous rate, with good stability for an extended period. Additionally, the wider range between the solidus and liquidus of the 6061 alloy, allows the material to obtain lower total viscosity at a wider range of temperatures and thus makes it less sensitive to temperature changes once frictional heating has brought the temperature of the material at the orifice to near its solidus.

This is presumption at this time, but we suspect that the material being plasticized near the internal orifice of the rotoforge tool must first obtain a temperature close to its solidus, perhaps between solidus and liquidus, to facilitate flow given the pressures we can provide with a basic FDM pinch wheel extruder. When a material is between its solidus and liquidus, it can behave as a semisolid material and its thixotropy becomes greatly enhanced... that is, it flows under lower applied stresses and its flowability increase with greater sensitivity to the rate of the applied stress.

Finally, we have found that the use of molybdenum disulfide and lithium greases on the inside of the hollow rotating motor shaft shaft and on the inside and outside of the PTFE and fiberglass shaft liners greatly aids in reducing material welding to the inside of the shaft and increases the maximum material feed rate any given alloy can sustain at a constant motor RPM. It also seems that the use of heavy grease greatly extends the lifetime of the liners... we also intend to try boron nitride spray, as it should provide even greater lubricity at higher temperatures and relative rotational velocities between liner, motor shaft and feed stock material. Only time and more experiments can tell what this will do for or against us.

All in all, it has been an exciting couple of weeks of experiments... things are getting close to functional, close enough that I am confident with some time and iteration we can find a solution that works and works well on the home desktop for less than 500 dollars...

Still, we have much to learn and much to try... Control and software still need a ton of work, but at least the hardware is becoming clearer.

If you made it with me this far, thanks for reading! I will be sure to add more detailed enegineering and science content on the challenges nad triumphs we face along the journey here on the rotoforge project in this blog... More than I can reasonably put in youtube videos or elsewhere so check back once and a while for more updates! Back to the lab!

Rotoforge 2023-11-30 Cold Working and Other Problems

 7 months of implementations later... I thought I grasped the physics. I was wrong. well not completely, but at least 50% wrong, which might...